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Researchers at the University of Córdoba have found that ion mobilÂity specÂtromÂeÂtry, comÂmonly used to detect exploÂsives and drugs at airÂports, can also effecÂtively idenÂtify fraudÂuÂlent olive oil, which is a major issue in the indusÂtry due to the lack of reliÂable anaÂlytÂiÂcal methÂods. The appliÂcaÂtion of this techÂnique could proÂvide a faster, more reliÂable way to deterÂmine if an olive oil is truly extra virÂgin, potenÂtially helpÂing to comÂbat fraud in the secÂtor.
Photo: waters.com
Researchers at the University of Córdoba have proven that ion mobilÂity specÂtromÂeÂtry, the anaÂlytÂiÂcal techÂnique most comÂmonly used to detect exploÂsives and drugs at airÂports, is also effecÂtive for idenÂtiÂfyÂing fraudÂuÂlent olive oil.
Olive oil falsely labelled as extra virÂgin is a major probÂlem in the olive oil secÂtor, with no one effecÂtive anaÂlytÂiÂcal method to idenÂtify and reveal fraud. Current analyÂses to deterÂmine if an olive oil is in fact extra virÂgin rely on senÂsory evalÂuÂaÂtion in conÂjuncÂtion with a numÂber of anaÂlytÂiÂcal tests, with no test deemed comÂpletely effecÂtive for detecÂtion.
Current chemÂiÂcal tests, includÂing deterÂmiÂnaÂtion of free acidÂity, perÂoxÂide value, wax conÂtent, fatty acid, sterol, and triglycÂeride comÂpoÂsiÂtion, are often inefÂfecÂtive in detectÂing adulÂterÂated oils. These oils are typÂiÂcally mixed with lower grade olive oils which have been chemÂiÂcally deodorÂized, makÂing them difÂfiÂcult to idenÂtify.
Federal food and drug guideÂlines state that to be labeled as extra virÂgin, the oil must be low acidÂity, comÂprise entirely of oil from the olive fruit and be cold pressed. The oil must also undergo a series of chemÂiÂcal and senÂsory tests.
The appliÂcaÂtion of ion mobilÂity specÂtromÂeÂtry, used to idenÂtify exploÂsives in both airÂports and milÂiÂtary use, is curÂrently being invesÂtiÂgated for use in a wide variÂety of areas in the agriÂculÂture and food secÂtors. The techÂnique is thought to have potenÂtial in deterÂminÂing the freshÂness of fish, disÂtinÂguishÂing between white wines and proÂvidÂing more accuÂrate deterÂmiÂnaÂtion of olive oil as extra virÂgin.
The techÂnique has been proÂposed for use as a screenÂing sysÂtem when applied to the olive secÂtor to allow quick, easy, and ecoÂnomÂiÂcal analyÂsis of oil samÂples to deterÂmine their catÂeÂgory. The process involves the heatÂing of one gram of oil in a vial to 60 degrees Celsius and genÂerÂatÂing volatile comÂpounds, which can then be sepÂaÂrated by size, charge, and mass. These are anaÂlyzed to proÂduce a specÂtrum, which can be interÂpreted to deterÂmine if the oil is extra virÂgin or not.
With the whole process takÂing around fifÂteen minÂutes per samÂple, the new approach to idenÂtiÂfiÂcaÂtion is sigÂnifÂiÂcantly faster than curÂrent methÂods which can take around eight hours. This time savÂing, along with the lack of need for samÂple preÂtreatÂment and the 90 perÂcent reliÂaÂbilÂity of the techÂnique, could make it an attracÂtive option to help with the issue of fraud in the secÂtor.